ABSTRACT This thesis aimed at the production of biolubricant from vegetable oils. The first stage produced methyl ester of the oil and in the second stage; the methyl ester was transesterified with Trimethylolpropane (TMP) in a ratio of 3.5:1 at 1500C to produce the biolubricant. The pour points biolubricant and its blend were significantly... Continue Reading

ABSTRACT This project was carried out using coal sample from Onyeama coal mine Enugu, Enugu State. Activated coal was produced by carbonizing the coal and activating it using phosphoric acid at a temperature of 5500c. the degree of bleaching of raw palm oil was monitored using spectronic meter through... Continue Reading

ABSTRACT This project was carried out using coal sample from Onyeama coal mine Enugu, Enugu State. Activated coal was produced by carbonizing the coal and activating it using phosphoric acid at a temperature of 5500c.  the degree of bleaching of raw palm oil was monitored using spectronic meter through absorbance measurement.  The essence was... Continue Reading

Metal complexes are scientifically known to be active and effective as antibacterial, antivirus and some antifungal etc. This project work is targeted at preparing complex from transition metals say; cobalt, cupper, zinc and nickel and organic ligands synthesised from pyridyl based schiff bases, one from 2-aminopyridine and benzaldehyde and second... Continue Reading

Metal complexes are scientifically known to be active and effective as antibacterial, antivirus and some antifungal etc. This project work is targeted at preparing complex from transition metals say; cobalt, cupper, zinc and nickel and organic ligands synthesised from pyridyl based schiff bases, one from 2-aminopyridine and benzaldehyde and second... Continue Reading

ABSTRACT Zinc Oxide (ZnO) nanowires with hexagonal structure were successfully synthesized by chemical bath deposition technique. The obtained nanowires were characterized by scanning electron microscope (SEM), X-ray diffraction (XRD), energy dispersive X-ray analysis (EDX) and spectrophotometer. The SEM micrographs revealed the morphology of ZnO... Continue Reading

ABSTRACT According to a few recent studies, calcium titanate is a material that is similar to hydroxyapatite in biological properties. However, calcium titanate is not currently being used in the biomedical application as to hydroxyapatite. The objective is to prepare nano calcium titanate powder from the solution of calcium oxide, ethanol, and... Continue Reading

ABSTRACT According to a few recent studies, calcium titanate is a material that is similar to hydroxyapatite in biological properties. However, calcium titanate is not currently being used in the biomedical application as to hydroxyapatite. The objective is to prepare nano calcium titanate powder from the solution of calcium oxide, ethanol, and... Continue Reading

ABSTRACT This project was carried out using coal sample from Onyeama coal mine Enugu, Enugu State.Activated coal was produced by carbonizing the coal and activating it using phosphoric acid at a temperature of 5500c. the degree of bleaching of raw palm oil was monitored using spectronic meter through absorbance measurement. The essence was to... Continue Reading

TABLE OF CONTENT Pages Title Page i Certification ii Dedication iii Acknowledgements iv Table of Contents v Abstract vii CHAPTER ONE 1.0 Introduction/Background of Study 1 1.1 Aim 4 1.2 Statement of Research Objective 4 1.3 Scope of Study 5 1.4 Literature Review 5 1.4.1 Structure and Composition of Lignocellulose Biomass 6 1.4.2 Cellulose 6 1.4.3... Continue Reading

TABLE OF CONTENT            Pages  Title Page                                                                                                 i  Certification                                                                                         ... Continue Reading

ABSTRACT Core-shell oxide thin films of TiO2/MnO, TiO2/CoO, TiO2/NiO and TiO2/CuO have been successfully synthesized and deposited on glass substrates, using the chemical bath deposition [CDB] technique. To ensure uniform coating, surface pre-treatment was carried out by cleaning slides with detergent, deionised water, ammonia acid and rinsed with... Continue Reading

ABSTRACT The synthesis of N-heteroaryl substituted benzene sulphonamides and evaluation of their biological activities are reported. Synthesis was achieved by the reaction of benzene sulphonyl chloride and substituted amino heterocycle in dry pyridine. The structures of synthesized compounds were assigned by spectroscopic methods. The eight (8)... Continue Reading

ABSTRACT The removal of Pb(II) ions from aqueous model solution using zeolite has been investigated under different operational parameters like heavy metal ion concentration, adsorbent amount and particle size. The zeolite used was synthesized and characterized using SEM and XRD analysis. The equilibrium adsorption capacity of zeolite used for... Continue Reading

ABSTRACT Electrochemical capacitors (ECs) or Super capacitors (SCs) are energy saving devices which have excellent properties that include high power density, long cycle life, low temperature sensitivity and low maintenance cost. However, these devices have lower energy densities than conventional batteries. To improve on its energy density, SnO2... Continue Reading

ABSTRACT The usefulness of non-steroidal anti-inflammatory agents in the management of rheumatoid diseases cannot be over-emphasized. As this disease is characterized by chronic inflammation, it is usual to test compounds for anti-inflammatory activity in animals and then hope that the active ones should be clinically useful as anti-rheumatic... Continue Reading

ABSTRACT The present paper describes the synthesis of Acid Orange(7)dye which can be used as dyes for cellulose acetate biopolymer. They were obtained by the diazotization of a monoazo component of the mono-azobenzene type, followed by coupling. The monoazo components were obtained by the diazotization of sulphanilic acid and coupling with... Continue Reading

ABSTRACT The present paper describes the synthesis of Acid Orange(7)dye which can be used as dyes for cellulose acetate biopolymer. They were obtained by the diazotization of a monoazo component of the mono-azobenzene type, followed by coupling. The monoazo components were obtained by the diazotization of sulphanilic acid and coupling with... Continue Reading

ABSTRACT In this study, a series of N-pyridin-3-yl substituted [phenylsulphonamido] acetamide has been synthesized. The reaction of phenylsulphonyl chloride with various amino acids in basic medium yielded phenylsulphonamido alkanoic acid which, on chlorination with thionyl chloride, gave acid chloride derivatives of phenylsulphonamido alkanoic... Continue Reading

Mechanochemical synthesis of  [Cu(OOCCH3)2(THB)2] and the Mechanochemical synthesis of  [Cu(OOCCH3)2(THB)2] were carried out, and a  brown solid complexes obtained in both experiment was washed in ethanol respectively. The  physical and instrumental characterisation of the complexes carried out revealed that the complexes obtained are the same... Continue Reading